glucose nmr assignment

D-(+)-Glucose (C6H12O6)

View large 3d structure, bmrb entry bmse000015.

Entry DOI : doi:10.13018/BMSE000015 Data source : Madison Metabolomics Consortium - Francisca Jofre, Mark E. Anderson, John L. Markley

NMR-STAR file :

Structure file (mol/sdf) :

All files for

Time Domain Data :

View the GISSMO record for this entry.

Sample and instrument details are given with the spectrum

Assigned chemical shifts

Set 1 Sample: multiple; see NMR-STAR file Conditions: temperature: 298K, pH: 7.4 Spectrometer: multiple; see NMR-STAR file

NMR experiments

1: 1D 1H, 0.5 mM Sample: 0.5mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

2: 1D 1H, 2.0 mM Sample: 2.0mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

3: 1D 1H Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

4: 2D [1H,1H]-TOCSY Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

5: 1D 13C Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

6: 1D DEPT90 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

7: 1D DEPT135 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

8: 2D [1H,13C]-HSQC Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

9: 2D [1H,13C]-HMBC Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

10: 2D [1H,1H]-COSY Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz

11: 2D [1H,13C]-HSQC SW small Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz